Quotation from: General Science

Written by: Bertha M. Clark


The best laboratory method of securing free chlorine is to heat in a
water bath a mixture of hydrochloric acid and manganese dioxide, a
compound containing one part of manganese and two parts of oxygen. The
heat causes the manganese dioxide to give up its oxygen, which
immediately combines with the hydrogen of the hydrochloric acid and
forms water. The manganese itself combines with part of the chlorine
originally in the acid, but not with all. There is thus some free
chlorine left over from the acid, and this passes off as a gas and can
be collected, as in Figure 158. Free chlorine is heavier than air, and
hence when it leaves the exit tube it settles at the bottom of the
jar, displacing the air, and finally filling the bottle.

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